Physical Metallurgy and Materials Engineering

Equipements

Research themes

Fatigue damage

Ongoing projects

Completed projects

Documents

Thermodynamique et défauts ponctuels (ADPI)
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UMET - Métallurgie Physique et Génie des Matériaux

Physical Metallurgy and Materials Engineering - Scientific instruments

Scientific instruments from the UMET instrument database managed by the research group.

3D optical profiler (ContourGT-K 3D Optical Microscope)

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

Profilometric measurements by non-contact optical microscope type 3D optical interferometric profilometer for reflective or non-reflective materials

Technical characteristics

Measuring range: 2.3mm² to 30μm.
Lateral resolution: up to 300 nm
Resolution in z: below the nm

Atomic Force Microscope Dimension 3100

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

Mode: Tapping / contact
Scanners: 90μm x 90μm x-y images, 6μm in vertical imaging (roughness)
Accessories :

Anti-vibration table
Sample holder: standard 150 mm chuck.
Motorized displacement plate (x, y): probed area 125mm x 100mm.
MFM mode

Atomic Force Microscope Multimode

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

AFM Multimode from Veeco
Technical characteristics

Contact mode
150μm x 150μm image
Vertical scale: 5 μm (roughness)

Chamber furnace (1750°C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

glass synthesis and high temperature annealing

cryogenic mill (CryoMill RETSCH)

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Vibrating mill, room temperature or liquid nitrogen temperature (77K)

Dilatometer DIL 402C

Research team: Métallurgie physique et génie des matériaux.

Contact: Rajashekhara SHABADI.

Vacuum dilatometer or neutral gas sweeping
Ambient temperature at 1500 ° C

Fatigue machine +/- 50 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 50 kN with furnace

Fatigue tests on metal test piece

fatigue machine with tubular furnace

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 250 kN, furnace max 650°C and possibility induction furnace.
Fatigue tests on metal test pieces up to 10 mm diameter

Flash DSC2+ (Mettler Toledo)

Research team: Métallurgie physique et génie des matériaux.

Contact: Marie-Noëlle Avettand-Fénoël.

Range of Temperature : T ambient at 1000 °C
Heating rate: 30 K / s to 40000 K/s
Cooling speed in absolute value up to 4000 K/s

Forced air annealing furnace (800 ° C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Forced air chamber furnace for non-reducing atmosphere annealing

High temperatue differential scanning calorimetry

Research team: Métallurgie physique et génie des matériaux.

Contact: Rajashekhara SHABADI.

High temperature furnace- 700-1500 ° C
Low temperature furnace (
Possibility of thermal cycling and simulation of rapid cooling
Ability to analyze samples under He, Ar and / or N2

hot enrobing press

Research team: Métallurgie physique et génie des matériaux.

Contacts: Damien CRETON, Matthieu TOUZIN.

Hot enrobing of sample in conductive or non-conductive resins
Coating diameter 30mm,
Enrobing parameters

Pressure from 50 to 350 bar in increments of 25 bar
Heating time From 1 to 15 minutes. in steps of 0.5 minutes.
Heating temperature 80-180 ° C in increments of 5 ° C
Cooling time From 1 to 15 min in steps of 0.5 min.

Hot press sintering

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Instron 4507, 200 kN cell
Graphite furnace HT 2000 ° C under secondary vacuum or neutral atmosphere (N2, Ar, He, ...)

low-pressure plasma system

Research teams: Ingénierie des systèmes polymères, Métallurgie physique et génie des matériaux.

Contact: Jean-François BRUN.

Low-pressure plasma system with a 40kHz/100W generator for

cleaning the surface of most of materials, including the smallest cracks
activating the surface to increase wettability

Treatment of small samples (a few cm2 or cm3)

Gaz available: air, pure oxygen.

Mössbauer Spectrometry

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Devices

57Co sources for the study of alloys containing iron;
1 spectrometer for measurements in ambient transmission;
1 spectrometer for reflection measurements at ambient temperature:

in CEMS mode - 0.2 μm;
in CXMS mode - 2 μm.

Possible Mössbauer studies

Identification and determination of phases, determination of their chemical composition;
Oxidation state of iron;
Local atomic order and local symmetry;
Properties: magnetic resolution, indication on charge transfer.

Analyzable materials

Powder, solid, sheet or coating on solid;
Nature: Steels (with nitrogen) coated (or not), minerals, catalysts, semiconductors.

Machine fatigue MTS 100 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 100 kN with tubular furnace 650 ° C or mechanical test in liquid nitrogen
Fatigue tests on metal specimen diameter (10 mm) hot or cold

Machine fatigue MTS 25 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 25 kN
Fatigue tests on small diameter metal specimen (4mm) and thin thickness (of the order of 0.350 mm)

Metal Fusion Platform

Research team: Métallurgie physique et génie des matériaux.

Contact: David BALLOY.

Development of induction platforms with ATYS Consulting Group

Induction furnace 25kW CEIA

     Direct and indirect heating
     Up to 20kg of steel

Resistance Tilting furnace12kW

     10 liters (Al foundry + galvanizing)

+ 1 liter tilting furnace

Micro-indenter MHT CSM Instruments

Research team: Métallurgie physique et génie des matériaux.

Contact: Matthieu TOUZIN.

Instrumented indentation (simultaneous recording of force and displacement) for loads ranging from 0.05 to 10 N; not instrumented beyond (up to 30 N)
Motorized X-Y stage (positioning
Coupled optical observation
Vickers type diamond indenter
Heated sample plate (up to 450 ° C)

mills SPEX 8000 (high energy grinding at ambient temperature)

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Possible programming of the duration and grinding cycle;

Container volume about 45 cm3;

grinding vials and balls in steel or alumina

Ovens under vacuum (250°C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Oven able to work under primary vacuum.
Capacity 65 l
Max temperature 250°C

planetary mill (Fritsch)

Research team: Métallurgie physique et génie des matériaux.

Contact: Marie-Noëlle Avettand-Fénoël.

Planetary mill used for metalls and mechanical alloying.

planetary mill (PM 100 Retsch)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Matthieu TOUZIN, Franck BéCLIN.

Planetary mill used for powder metallurgy of ceramic and metal . Mechanical alloying of metals.

Volume of milling jars up to 500 ml.

Possible programming of the duration, the speed and the grinding cycle;
Speed up to 600 rpm;
Bowls and balls in stainless steel, tungsten carbide, agate and alumina.

Rolling mill

Research team: Métallurgie physique et génie des matériaux.

Contacts: David BALLOY, Matthieu TOUZIN.

Mini electric rolling mill
Maximum opening between cylinders: 37 mm
Hot rolling (preheating oven up to 1200 ° C - atmo N2)
Cold rolling

tensile test device +/- 30 kN with +/- 30 kN controlled atmosphere test chamber +/- 30 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / tensile test 30 kN
Tensile tests or Small Punch Test at temperature up to 500 ° C (heating cord) with control of the oxygen content and moisture content

Tensile test device +/- 30kN INSTRON 5567A

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / tensile test 30 kN

Tensile tests or Small Punch Test at temperature up to 500 ° C (heating cord)

Vibration polisher VibroMet 2 BUEHLER

Research team: Métallurgie physique et génie des matériaux.

Contact: Damien CRETON.

Finishing polishing with colloidal silica on a wide range of materials, especially for EBSD applications

Unité Matériaux et Transformations
CNRS UMR 8207 - Université de Lille

Unité Matériaux et Transformations
CNRS UMR 8207 - Université de Lille

Unité Matériaux et Transformations
CNRS UMR 8207 - Université de Lille